PittsburghV1, Main, Exploration, bibRecord, 000720

Growth of Ca2MnO4 Ruddlesden-Popper structured thin films using Combinatorial Substrate Epitaxy

Identifieur interne : 000720 ( Main/Exploration ); précédent : 000719; suivant : 000721

Growth of Ca2MnO4 Ruddlesden-Popper structured thin films using Combinatorial Substrate Epitaxy

Auteurs : Morgane Lacotte [France] ; Adrien David [France] ; Dhanapal Pravarthana [France] ; Clara Grygiel [France] ; Gregory S. Rohrer [États-Unis] ; Paul A. Salvador [États-Unis] ; Matias Velázquez [France] ; K. De Kloe [Pays-Bas] ; Wilfrid Prellier [France]

Source :

Journal of Applied Physics [ 0021-8979 ] ; 2014.

RBID : Hal:hal-01101849

Abstract

The local epitaxial growth of pulsed laser deposited Ca$_2$MnO$_4$ films on polycrystalline spark plasma sintered Sr$_2$TiO$_4$ substrates was investigated to determine phase formation and preferred epitaxial orientation relationships ($ORs$) for isostructural Ruddlesden-Popper (RP) heteroepitaxy, further developing the high-throughput synthetic approach called Combinatorial Substrate Epitaxy (CSE). Both grazing incidence X-ray diffraction and electron backscatter diffraction (EBSD) patterns of the film and substrate were indexable as single-phase RP-structured compounds. The optimal growth temperature (between 650 $^{\circ}$C and 800 $^{\circ}$C) was found to be 750 $^{\circ}$C using the maximum value of the average image quality (IQ) of the backscattered diffraction patterns. Films grew in a grain-over-grain pattern such that each Ca$_2$MnO$_4$ grain had a single $OR$ with the Sr$_2$TiO$_4$ grain on which it grew. Three primary $ORs$ described 47 out of 49 grain pairs that covered nearly all of RP orientation space. The first $OR$, found for 20 of the 49, was the expected RP unit-cell over RP unit-cell $OR$, expressed as [100][001]$_{film}$||[100][001]$_{sub}$. The other two $ORs$ were essentially rotated from the first by 90$^{\circ}$, with one (observed for 17 of 49 pairs) being rotated about the [100] and the other (observed for 10 of 49 pairs) being rotated about the [110] (and not exactly by 90$^{\circ}$). These results indicate that only a small number of $ORs$ are needed to describe isostructural RP heteroepitaxy and further demonstrate the potential of CSE in the design and growth of a wide range of complex functional oxides.

Url:

https://hal.archives-ouvertes.fr/hal-01101849

DOI: 10.1063/1.4905012

Affiliations:

Links toward previous steps (curation, corpus...)

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Le document en format XML

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<country>France</country>
<placeName><settlement type="city">Bordeaux</settlement>
<region type="region" nuts="2">Nouvelle-Aquitaine</region>
<region type="old region" nuts="2">Aquitaine</region>
</placeName>
<orgName type="university">Université de Bordeaux</orgName>
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<author><name sortKey="De Kloe, K" sort="De Kloe, K" uniqKey="De Kloe K" first="K." last="De Kloe">K. De Kloe</name>
<affiliation wicri:level="1"><hal:affiliation type="laboratory" xml:id="struct-410079" status="INCOMING">          <orgName>EDAX Application Laboratory</orgName>
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</hal:affiliation>
<country>Pays-Bas</country>
</affiliation>
</author>
<author><name sortKey="Prellier, Wilfrid" sort="Prellier, Wilfrid" uniqKey="Prellier W" first="Wilfrid" last="Prellier">Wilfrid Prellier</name>
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          <orgName type="acronym">CRISMAT</orgName>
          <desc>            <address>              <addrLine>6 Bvd du maréchal Juin 14050 CAEN CEDEX 4</addrLine>
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          <orgName>Université de Caen Normandie</orgName>
          <orgName type="acronym">UNICAEN</orgName>
          <date type="start">1432</date>
          <desc>            <address>              <addrLine>Esplanade de la Paix - CS 14032 - 14032 CAEN Cedex 5</addrLine>
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          <orgName>Normandie Université</orgName>
          <orgName type="acronym">NU</orgName>
          <date type="start">2015-01-01</date>
          <desc>            <address>              <addrLine>Esplanade de la Paix - CS 14032 - 14032 Caen Cedex 5</addrLine>
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          <desc>            <address>              <addrLine>6, Boulevard du Maréchal Juin CS 45053 14050 CAEN cedex 04</addrLine>
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          <orgName>Centre National de la Recherche Scientifique</orgName>
          <orgName type="acronym">CNRS</orgName>
          <date type="start">1939-10-19</date>
          <desc>            <address>              <country key="FR"></country>
            </address>
            <ref type="url">http://www.cnrs.fr/</ref>
          </desc>
        </org>
</tutelle>
</tutelles>
</hal:affiliation>
<country>France</country>
</affiliation>
</author>
</analytic>
<idno type="DOI">10.1063/1.4905012</idno>
<series><title level="j">Journal of Applied Physics</title>
<idno type="ISSN">0021-8979</idno>
<imprint><date type="datePub">2014</date>
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<front><div type="abstract" xml:lang="en">The local epitaxial growth of pulsed laser deposited Ca$_2$MnO$_4$ films on polycrystalline spark plasma sintered Sr$_2$TiO$_4$ substrates was investigated to determine phase formation and preferred epitaxial orientation relationships ($ORs$) for isostructural Ruddlesden-Popper (RP) heteroepitaxy, further developing the high-throughput synthetic approach called Combinatorial Substrate Epitaxy (CSE). Both grazing incidence X-ray diffraction and electron backscatter diffraction (EBSD) patterns of the film and substrate were indexable as single-phase RP-structured compounds. The optimal growth temperature (between 650 $^{\circ}$C and 800 $^{\circ}$C) was found to be 750 $^{\circ}$C using the maximum value of the average image quality (IQ) of the backscattered diffraction patterns. Films grew in a grain-over-grain pattern such that each Ca$_2$MnO$_4$ grain had a single $OR$ with the Sr$_2$TiO$_4$ grain on which it grew. Three primary $ORs$ described 47 out of 49 grain pairs that covered nearly all of RP orientation space. The first $OR$, found for 20 of the 49, was the expected RP unit-cell over RP unit-cell $OR$, expressed as [100][001]$_{film}$||[100][001]$_{sub}$. The other two $ORs$ were essentially rotated from the first by 90$^{\circ}$, with one (observed for 17 of 49 pairs) being rotated about the [100] and the other (observed for 10 of 49 pairs) being rotated about the [110] (and not exactly by 90$^{\circ}$). These results indicate that only a small number of $ORs$ are needed to describe isostructural RP heteroepitaxy and further demonstrate the potential of CSE in the design and growth of a wide range of complex functional oxides.</div>
</front>
</TEI>
<affiliations><list><country><li>France</li>
<li>Pays-Bas</li>
<li>États-Unis</li>
</country>
<region><li>Aquitaine</li>
<li>Nouvelle-Aquitaine</li>
</region>
<settlement><li>Bordeaux</li>
</settlement>
<orgName><li>Université de Bordeaux</li>
</orgName>
</list>
<tree><country name="France"><noRegion><name sortKey="Lacotte, Morgane" sort="Lacotte, Morgane" uniqKey="Lacotte M" first="Morgane" last="Lacotte">Morgane Lacotte</name>
</noRegion>
<name sortKey="David, Adrien" sort="David, Adrien" uniqKey="David A" first="Adrien" last="David">Adrien David</name>
<name sortKey="Grygiel, Clara" sort="Grygiel, Clara" uniqKey="Grygiel C" first="Clara" last="Grygiel">Clara Grygiel</name>
<name sortKey="Pravarthana, Dhanapal" sort="Pravarthana, Dhanapal" uniqKey="Pravarthana D" first="Dhanapal" last="Pravarthana">Dhanapal Pravarthana</name>
<name sortKey="Prellier, Wilfrid" sort="Prellier, Wilfrid" uniqKey="Prellier W" first="Wilfrid" last="Prellier">Wilfrid Prellier</name>
<name sortKey="Velazquez, Matias" sort="Velazquez, Matias" uniqKey="Velazquez M" first="Matias" last="Velázquez">Matias Velázquez</name>
</country>
<country name="États-Unis"><noRegion><name sortKey="Rohrer, Gregory S" sort="Rohrer, Gregory S" uniqKey="Rohrer G" first="Gregory S." last="Rohrer">Gregory S. Rohrer</name>
</noRegion>
<name sortKey="Salvador, Paul A" sort="Salvador, Paul A" uniqKey="Salvador P" first="Paul A." last="Salvador">Paul A. Salvador</name>
</country>
<country name="Pays-Bas"><noRegion><name sortKey="De Kloe, K" sort="De Kloe, K" uniqKey="De Kloe K" first="K." last="De Kloe">K. De Kloe</name>
</noRegion>
</country>
</tree>
</affiliations>
</record>

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Growth of Ca2MnO4 Ruddlesden-Popper structured thin films using Combinatorial Substrate Epitaxy

Growth of Ca2MnO4 Ruddlesden-Popper structured thin films using Combinatorial Substrate Epitaxy

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